@article{HALL2020106778,
title = {A temperature-controlled sample shuttle for field-cycling NMR},
author = {Andrew M R Hall and Topaz A A Cartlidge and Giuseppe Pileio},
url = {http://www.sciencedirect.com/science/article/pii/S1090780720300963},
doi = {https://doi.org/10.1016/j.jmr.2020.106778},
issn = {1090-7807},
year = {2020},
date = {2020-01-01},
journal = {Journal of Magnetic Resonance},
pages = {106778},
abstract = {We present a design for a temperature-controlled sample shuttle for use in NMR measurements at variable magnetic field strength. Accurate temperature control was achieved using a mixture of water-ethylene glycol as a heat transfer fluid, reducing temperature gradients across the sample to \<0.05 °C and minimising convection. Using the sample shuttle, we show how the longitudinal (T1) and singlet order (TS) relaxation time constants were measured for two molecules capable of supporting long-lived states, with new record lifetimes observed at low field and above ambient temperatures.},
keywords = {},
pubstate = {published},
tppubtype = {article}
}
